New boron complex
New boron complex based on 3-(2-pyridyl)pyrazole Chelates
of bis(4-tert-butylphenyl): Synthesis and X-ray Crystal Structure
Adel M.
Najar1 and Mike D. Ward2
1. Faculty of Education, Chemistry Department, Univeristy
of Benghazi, Elmarj, Libya.
2. Department of Chemistry, University of Sheffield,
Sheffield, UK S3 7HF, UK
Abstract: The
synthesis and crystal structure of (Bt-BuPh2(3-(2-pyridyl)pyrazolate))
complex is described. The structure of the complex was determined by using
single crystal X-ray diffraction. The compound crystallized in symmetry cell
setting orthorhombic of P212121 with a = 11.067(2) Å, b =
11.202(2) Å, c = 20.542(4) Å and Z = 4. The structure of complex reveals that
the boron centre is four coordinated. The formed compound, emitting materials
which could be of interest for practical applications.
[Adel M. Najar, Mike D. Ward. New boron
complex based on 3-(2-pyridyl)pyrazole Chelates of bis(4-tert-butylphenyl):
Synthesis and X-ray Crystal Structure J Am Sci 2013;9(3):251-252]. (ISSN:
1545-1003). http://www.jofamericanscience.org. 34
Keywords: 3-(2-pyridyl)pyrazole; boron complex; crystal
structure. Full Text 34